7,7-Dichloro-1,6-dimethyl-2-oxa-5-thiabicyclo[4.1.0]heptane 5,5-dioxide and 6-chloro-2,3-dihydro-7-methyl-5-methylene-2<i>H</i>,3<i>H</i>,5<i>H</i>-1,4-dithiepine 1,1,4,4-tetraoxide
Authors of publication
Brewer, A. David; Ferguson, George; Znotins, Andrew A.
Journal of publication
Acta Crystallographica Section C
Year of publication
2000
Journal volume
56
Journal issue
3
Pages of publication
e109 - e110
a
11.2341 ± 0.0017 Å
b
6.8536 ± 0.0011 Å
c
13.0566 ± 0.0012 Å
α
90°
β
97.307 ± 0.009°
γ
90°
Cell volume
997.1 ± 0.2 Å3
Cell temperature
294 ± 1 K
Ambient diffraction temperature
294 ± 1 K
Number of distinct elements
5
Space group number
14
Hermann-Mauguin space group symbol
P 1 21/a 1
Hall space group symbol
-P 2yab
Residual factor for all reflections
0.042
Residual factor for significantly intense reflections
0.029
Weighted residual factors for all reflections included in the refinement
0.075
Goodness-of-fit parameter for all reflections included in the refinement