Crystallography Open Database
- COD Home
- Accessing COD Data
- Add Your Data
- Documentation
Information card for entry 2010897
Preview
Coordinates | 2010897.cif |
---|---|
Structure factors | 2010897.hkl |
Original IUCr paper | HTML |
Chemical name | Bis(μ-3,11-diethyl-6,8-diphenyl-3,6,8,11-tetraphosphatridecane- κ^4^-P^3^,P^6^:P^8^,P^11^)dirhodium(I) bis(tetrafluoroborate) |
---|---|
Formula | C50 H80 B2 F8 P8 Rh2 |
Calculated formula | C50 H80 B2 F8 P8 Rh2 |
SMILES | [Rh]123[P](CC[P]2(C[P]2([Rh]4([P](C[P]3(CC[P]1(CC)CC)c1ccccc1)(c1ccccc1)CC[P]4(CC)CC)[P](CC2)(CC)CC)c1ccccc1)c1ccccc1)(CC)CC.[B](F)(F)(F)[F-].[B](F)(F)(F)[F-] |
Title of publication | A binuclear rhodium(I) complex with two tetraphosphine ligands at 100K |
Authors of publication | Hunt Jr, Clinton; Nelson, Brent D.; Harmon, Elisa G.; Fronczek, Frank R.; Watkins, Steven F.; Billodeaux, Damon R.; Stanley, George G. |
Journal of publication | Acta Crystallographica Section C |
Year of publication | 2000 |
Journal volume | 56 |
Journal issue | 5 |
Pages of publication | 546 - 548 |
a | 15.651 ± 0.003 Å |
b | 16.048 ± 0.003 Å |
c | 24.022 ± 0.005 Å |
α | 90° |
β | 108.18 ± 0.03° |
γ | 90° |
Cell volume | 5732 ± 2 Å3 |
Cell temperature | 100 K |
Ambient diffraction temperature | 100 K |
Number of distinct elements | 6 |
Space group number | 9 |
Hermann-Mauguin space group symbol | C 1 c 1 |
Hall space group symbol | C -2yc |
Residual factor for all reflections | 0.049 |
Residual factor for significantly intense reflections | 0.038 |
Weighted residual factors for all reflections | 0.095 |
Weighted residual factors for significantly intense reflections | 0.089 |
Goodness-of-fit parameter for all reflections | 1.04 |
Goodness-of-fit parameter for significantly intense reflections | 1.03 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | Yes |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/2010897.html
All data in the COD and the database itself are dedicated to the
public domain and licensed under the
CC0
License
.
Users of the data should acknowledge the original authors of the
structural data.