Information card for entry 2010921

Structure parameters

• Formula: C12 H14 Br2 Cl2 N2 Si
• Calculated formula: C12 H14 Br2 Cl2 N2 Si
• Title of publication: Complexes of mixed silicon halides with 4-picoline
• Authors of publication: Hensen, Karl; Mayr-Stein, Ralf; Spangenberg, Björn; Bolte, Michael
• Journal of publication: Acta Crystallographica Section C
• Year of publication: 2000
• Journal volume: 56
• Journal issue: 5
• Pages of publication: 610 - 613
• a: 7.252 ± 0.002 Å
• b: 8.12 ± 0.002 Å
• c: 13.54 ± 0.003 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 797.3 ± 0.3 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 6
• Space group number: 53
• Hermann-Mauguin space group symbol: P m n a
• Hall space group symbol: -P 2ac 2
• Residual factor for all reflections: 0.0352
• Residual factor for significantly intense reflections: 0.0272
• Weighted residual factors for all reflections included in the refinement: 0.0634
• Goodness-of-fit parameter for all reflections included in the refinement: 1.119
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: Yes