Tetraallyl (2,2'-bipyridyl)-<i>rac</i>-3,3,7,7-tetramethyl-<i>trans</i>-5-palladatricyclo[4.1.0.0^2,^^4^]heptane-1,2,4,6-tetracarboxylate above and below the phase-transition temperature of 194K
Authors of publication
Bats, Jan W.; Rivas Nass, Andreas; Hashmi, A. Stephen K.
Journal of publication
Acta Crystallographica Section C
Year of publication
2000
Journal volume
56
Journal issue
7
Pages of publication
814 - 817
a
8.9583 ± 0.0008 Å
b
11.3245 ± 0.0018 Å
c
17.906 ± 0.003 Å
α
83.438 ± 0.016°
β
88.482 ± 0.014°
γ
72.118 ± 0.016°
Cell volume
1717.4 ± 0.5 Å3
Cell temperature
205 ± 2 K
Ambient diffraction temperature
205 ± 2 K
Number of distinct elements
5
Space group number
2
Hermann-Mauguin space group symbol
P -1
Hall space group symbol
-P 1
Residual factor for all reflections
0.0585
Residual factor for significantly intense reflections
0.0422
Weighted residual factors for all reflections included in the refinement
0.1009
Goodness-of-fit parameter for all reflections included in the refinement