Information card for entry 2011766

Structure parameters

• Chemical name: cis-Bis[N^1^,N^2^-bis(trimethylsilyl)benzamidinato-κ^2^N^1^N^2^]-chloro- (4-tolylimido-κN)-vanadium(V)
• Formula: C33 H53 Cl N5 Si4 V
• Calculated formula: C33 H53 Cl N5 Si4 V
• Title of publication: <i>cis</i>-Bis[<i>N</i>^1^,<i>N</i>^2^-bis(trimethylsilyl)benzamidinato-κ^2^<i>N</i>^1^,<i>N</i>^2^]chloro(4-tolylimido-κ<i>N</i>)vanadium(V)
• Authors of publication: Ellis, Dianne D.; Spek, Anthony L.
• Journal of publication: Acta Crystallographica Section C
• Year of publication: 2001
• Journal volume: 57
• Journal issue: 2
• Pages of publication: 147 - 148
• a: 10.16 ± 0.0005 Å
• b: 18.4257 ± 0.001 Å
• c: 22.643 ± 0.0013 Å
• α: 90°
• β: 109.808 ± 0.005°
• γ: 90°
• Cell volume: 3988.1 ± 0.4 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.102
• Residual factor for significantly intense reflections: 0.052
• Weighted residual factors for all reflections included in the refinement: 0.108
• Goodness-of-fit parameter for all reflections included in the refinement: 0.99
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: Yes