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Information card for entry 2012129
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Coordinates | 2012129.cif |
---|---|
Structure factors | 2012129.hkl |
Original IUCr paper | HTML |
Common name | [(PPh~3~)~2~PtB~10~H~11~-8-(OCH~3~)]0.5(CH~2~Cl~2~) |
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Chemical name | 8-methoxy-7,7-bis(triphenylphosphorine-P)- 8,9:10,11-di-μ-H-7-platina-nido-undecaborane dichloromethane hemisolvate |
Formula | C37.5 H45 B10 Cl O P2 Pt |
Calculated formula | C37.5 H45 B10 Cl O P2 Pt |
Title of publication | Three monoalkoxy-substituted <i>nido</i>-platinaboranes: [(PPh~3~)~2~PtB~10~H~11~-8-(OCH~3~)], [(PPh~3~)~2~PtB~10~H~11~-8-{OCH(CH~3~)~2~}] and [(PPh~3~)~2~PtB~10~H~10~-9-{OCH(CH~3~)~2~}] |
Authors of publication | Nie, Yong; Hu, Chun-Hua; Li, Xue; Yong, Wei; Dou, Jian Min; Sun, Jie; Jin, Ruo-Shui; Zheng, Pei-Ju |
Journal of publication | Acta Crystallographica Section C |
Year of publication | 2001 |
Journal volume | 57 |
Journal issue | 8 |
Pages of publication | 897 - 899 |
a | 12.85 ± 0.002 Å |
b | 25.824 ± 0.007 Å |
c | 13.308 ± 0.002 Å |
α | 90° |
β | 105.77 ± 0.01° |
γ | 90° |
Cell volume | 4249.9 ± 1.5 Å3 |
Cell temperature | 293 ± 2 K |
Ambient diffraction temperature | 293 ± 2 K |
Number of distinct elements | 7 |
Space group number | 14 |
Hermann-Mauguin space group symbol | P 1 21/n 1 |
Hall space group symbol | -P 2yn |
Residual factor for all reflections | 0.055 |
Residual factor for significantly intense reflections | 0.037 |
Weighted residual factors for all reflections included in the refinement | 0.105 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.04 |
Diffraction radiation wavelength | 0.71069 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | Yes |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/2012129.html
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