Information card for entry 2013008

Structure parameters

• Chemical name: propylammonium tris(2-aminoethyl)amine-1κ^4^N-di-μ-thio-1:2κ^4^S-dithio- 2κ^2^S-antimony(V)nickel(II)
• Formula: C9 H28 N5 Ni S4 Sb
• Calculated formula: C9 H28 N5 Ni S4 Sb
• SMILES: [Sb](=S)([S-])(S1)S[Ni]1234[N](CC[NH2]2)(CC[NH2]3)CC[NH2]4.[NH3+]CCC
• Title of publication: The new thioantimonate(V) (C~3~H~10~N)[NiSbS~4~(C~6~H~18~N~4~)]
• Authors of publication: Ralph Stähler; Wolfgang Bensch
• Journal of publication: Acta Crystallographica Section C
• Year of publication: 2002
• Journal volume: 58
• Journal issue: 11
• Pages of publication: m537 - m538
• a: 7.5707 ± 0.0015 Å
• b: 11.303 ± 0.002 Å
• c: 12.605 ± 0.003 Å
• α: 63.98 ± 0.03°
• β: 84.49 ± 0.03°
• γ: 82.26 ± 0.03°
• Cell volume: 959.6 ± 0.4 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.031
• Residual factor for significantly intense reflections: 0.019
• Weighted residual factors for significantly intense reflections: 0.047
• Weighted residual factors for all reflections included in the refinement: 0.05
• Goodness-of-fit parameter for all reflections included in the refinement: 1.017
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: Yes