Information card for entry 2013067

Structure parameters

• Formula: C24 H24 N10 Ni O6
• Calculated formula: C24 H24 N10 Ni O6
• SMILES: CN1O[Ni]2([N](c3ccc(N(=O)=O)cc3)=N1)([n]1ccccc1)(ON(C)N=[N]2c1ccc(N(=O)=O)cc1)[n]1ccccc1
• Title of publication: <i>trans</i>-Bis[1-methyl-3-(<i>p</i>-nitrophenyl)triazenido 1-oxide-κ^2^<i>N</i>^3^,<i>O</i>]dipyridinenickel(II)
• Authors of publication: Hörner, Manfredo; Oliveira, Julieta Saldanha de; Bordinhao, Jairo; Beck, Johannes
• Journal of publication: Acta Crystallographica Section C
• Year of publication: 2002
• Journal volume: 58
• Journal issue: 12
• Pages of publication: m586 - m587
• a: 10.473 ± 0.002 Å
• b: 14.961 ± 0.003 Å
• c: 8.569 ± 0.002 Å
• α: 90°
• β: 94.028 ± 0.01°
• γ: 90°
• Cell volume: 1339.3 ± 0.5 ų
• Cell temperature: 294 ± 1 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0465
• Residual factor for significantly intense reflections: 0.0311
• Weighted residual factors for significantly intense reflections: 0.0699
• Weighted residual factors for all reflections included in the refinement: 0.0763
• Goodness-of-fit parameter for all reflections included in the refinement: 1.033
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: Yes