<i>N</i>-Fluoropyridinium trifluoromethanesulfonate and 1-fluoro-2,4,6-trimethoxy-1,3,5-triazinium hexafluoroantimonate: the first experimental determination of the F—N^+^ bond length involving <i>sp</i>^2^ nitrogen
Authors of publication
Banks, R. Eric; Besheesh, Mohamed K.; Pritchard, Robin G.; 1-fluoro-2,4,6-trimethoxy-1,3,5-triazinium hexafluoroantimonate
Journal of publication
Acta Crystallographica Section C
Year of publication
2003
Journal volume
59
Journal issue
4
Pages of publication
m141 - m143
a
7.616 ± 0.002 Å
b
11.843 ± 0.003 Å
c
14.924 ± 0.003 Å
α
90°
β
97.43 ± 0.02°
γ
90°
Cell volume
1334.8 ± 0.6 Å3
Cell temperature
203 ± 2 K
Number of distinct elements
6
Space group number
14
Hermann-Mauguin space group symbol
P 1 21/n 1
Hall space group symbol
-P 2yn
Residual factor for significantly intense reflections
0.034
Weighted residual factors for all reflections included in the refinement
0.071
Goodness-of-fit parameter for all reflections included in the refinement
