Information card for entry 2013688

Structure parameters

• Formula: C49.196 H24 B Cl6.392 D2.392 F20 Li N4 Pd2
• Calculated formula: C49.196 H25.274 B Cl6.392 D1.118 F20 Li N4 Pd2
• Title of publication: Tetra-μ-chloro-1:2κ^4^<i>Cl</i>;1:3κ^4^<i>Cl</i>-bis(4,4'-dimethyl-2,2'-bipyridine)-2κ^2^<i>N</i>,3κ^2^<i>N</i>-lithium(I)dipalladium(II) tetrakis(pentafluorophenyl)borate dichloromethane 1.196-solvate
• Authors of publication: Han Shen; Ian M. Steele; Richard F. Jordan
• Journal of publication: Acta Crystallographica Section C
• Year of publication: 2003
• Journal volume: 59
• Journal issue: 10
• Pages of publication: m405 - m406
• a: 22.361 ± 0.006 Å
• b: 7.939 ± 0.002 Å
• c: 31.754 ± 0.009 Å
• α: 90°
• β: 98.621 ± 0.005°
• γ: 90°
• Cell volume: 5573 ± 3 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 9
• Space group number: 13
• Hermann-Mauguin space group symbol: P 1 2/c 1
• Hall space group symbol: -P 2yc
• Residual factor for all reflections: 0.083
• Residual factor for significantly intense reflections: 0.0764
• Weighted residual factors for significantly intense reflections: 0.1783
• Weighted residual factors for all reflections included in the refinement: 0.1817
• Goodness-of-fit parameter for all reflections included in the refinement: 1.246
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: Yes