2,4-Difluorobenzaldehyde benzoylhydrazone and 2,4-dichlorobenzaldehyde benzoylhydrazone are isostructural at 120K with <i>Z</i>' = 2: complex sheets built from N—H···O, C—H···O and C—H···π(arene) hydrogen bonds
Authors of publication
Wardell, Solange M. S. V.; de Lima Ferreira, Marcelle; de Souza, Marcus V. N.; Wardell, James L.; Low, John N.; Glidewell, Christopher
Journal of publication
Acta Crystallographica Section C
Year of publication
2006
Journal volume
62
Journal issue
3
Pages of publication
o118 - o121
a
10.5093 ± 0.0005 Å
b
17.6499 ± 0.0009 Å
c
14.7982 ± 0.0005 Å
α
90°
β
104.732 ± 0.002°
γ
90°
Cell volume
2654.7 ± 0.2 Å3
Cell temperature
120 ± 2 K
Ambient diffraction temperature
120 ± 2 K
Number of distinct elements
5
Space group number
14
Hermann-Mauguin space group symbol
P 1 21/n 1
Hall space group symbol
-P 2yn
Residual factor for all reflections
0.1182
Residual factor for significantly intense reflections
0.061
Weighted residual factors for significantly intense reflections
0.1343
Weighted residual factors for all reflections included in the refinement
0.155
Goodness-of-fit parameter for all reflections included in the refinement