Information card for entry 2014509

Structure parameters

• Chemical name: Dibromotetra-μ~2~-methoxo-di-μ~3~-methoxo-hexakis(tetrahydrofuran-d~8~- κO)tetramagnesium
• Formula: C30 H18 Br2 D48 Mg4 O12
• Calculated formula: C30 H66 Br2 Mg4 O12
• Title of publication: Dibromotetra-μ~3~-methoxo-di-μ~2~-methoxo-hexakis(tetrahydrofuran-<i>d</i>~8~)tetramagnesium
• Authors of publication: Walfort, Bernhard; Yousef, Rushdi I.; Rüffer, Tobias; Steinborn, Dirk
• Journal of publication: Acta Crystallographica Section C
• Year of publication: 2004
• Journal volume: 60
• Journal issue: 10
• Pages of publication: m482 - m483
• a: 8.4836 ± 0.0004 Å
• b: 18.9094 ± 0.0009 Å
• c: 12.8907 ± 0.0006 Å
• α: 90°
• β: 97.457 ± 0.001°
• γ: 90°
• Cell volume: 2050.43 ± 0.17 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0513
• Residual factor for significantly intense reflections: 0.0368
• Weighted residual factors for significantly intense reflections: 0.0914
• Weighted residual factors for all reflections included in the refinement: 0.099
• Goodness-of-fit parameter for all reflections included in the refinement: 1.029
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: Yes