Information card for entry 2014703

Structure parameters

• Chemical name: poly[[tris[(5,12-dimethyl-7,14-diphenyl-1,4,8,11-tetracyclotetradiene)copper(II)]-tri-μ-cyamo-bis[tricyanocobalt(III)]]dimethylformamide solvate trihydrate]
• Formula: C87 H109 Co2 Cu3 N25 O4
• Calculated formula: C87 H109 Co2 Cu3 N25 O4
• Title of publication: Cyano-bridged extended heteronuclear supramolecular architectures with hexacyanocobalt(III) as building blocks
• Authors of publication: Li, Yan-Ping; Yang, Pin; Huang, Zi-Xiang; Xie, Fu-Xin
• Journal of publication: Acta Crystallographica Section C
• Year of publication: 2005
• Journal volume: 61
• Journal issue: 3
• Pages of publication: m122 - m124
• a: 9.251 ± 0.0003 Å
• b: 16.4054 ± 0.0005 Å
• c: 17.8005 ± 0.0005 Å
• α: 113.016 ± 0.001°
• β: 93.684 ± 0.001°
• γ: 101.966 ± 0.001°
• Cell volume: 2400.55 ± 0.13 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0938
• Residual factor for significantly intense reflections: 0.0755
• Weighted residual factors for significantly intense reflections: 0.1873
• Weighted residual factors for all reflections included in the refinement: 0.2004
• Goodness-of-fit parameter for all reflections included in the refinement: 1.094
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: Yes