Information card for entry 2014798

Structure parameters

• Common name: cis-Co(en)2(N3)2 picrate
• Chemical name: cis-diazidobis(ethylenediamine-κ^2^N,N')cobalt(III) picrate
• Formula: C10 H18 Co N13 O7
• Calculated formula: C10 H18 Co N13 O7
• SMILES: [Co]12(N=N#N)(N=N#N)([NH2]CC[NH2]1)[NH2]CC[NH2]2.[O-]c1c(cc(N(=O)=O)cc1N(=O)=O)N(=O)=O
• Title of publication: Second-sphere coordination in anion binding: <i>cis</i>-diazidobis(ethylenediamine-κ^2^<i>N</i>,<i>N</i>')cobalt(III) picrate
• Authors of publication: Sharma, Raj Pal; Sharma, Rajni; Bala, Ritu; Bond, Andrew D.
• Journal of publication: Acta Crystallographica Section C
• Year of publication: 2005
• Journal volume: 61
• Journal issue: 6
• Pages of publication: m272 - m274
• a: 9.1229 ± 0.0003 Å
• b: 12.098 ± 0.0005 Å
• c: 32.8793 ± 0.0012 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 3628.9 ± 0.2 ų
• Cell temperature: 180 ± 2 K
• Ambient diffraction temperature: 180 ± 2 K
• Number of distinct elements: 5
• Space group number: 61
• Hermann-Mauguin space group symbol: P b c a
• Hall space group symbol: -P 2ac 2ab
• Residual factor for all reflections: 0.0503
• Residual factor for significantly intense reflections: 0.0423
• Weighted residual factors for significantly intense reflections: 0.1111
• Weighted residual factors for all reflections included in the refinement: 0.1152
• Goodness-of-fit parameter for all reflections included in the refinement: 1.04
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: Yes