The (1<i>RS</i>,2<i>RS</i>,7<i>RS</i>,8<i>RS</i>)- and (1<i>RS</i>,2<i>SR</i>,7<i>SR</i>,8<i>RS</i>)-diastereoisomers of 8,9,11,12-tetrachloro-<i>N</i>-ethyltricyclo[6.2.2.0^2,7^]dodeca-9,11-diene-1,10-dicarboximide
Authors of publication
Grimley, Fionuala M.; O'Donnell, Cormac; Pratt, Albert C.; Long, Conor; Howie, R. Alan
Journal of publication
Acta Crystallographica Section C
Year of publication
2005
Journal volume
61
Journal issue
6
Pages of publication
o369 - o372
a
10.937 ± 0.007 Å
b
9.228 ± 0.004 Å
c
17.1 ± 0.006 Å
α
90°
β
94.83 ± 0.04°
γ
90°
Cell volume
1719.7 ± 1.5 Å3
Cell temperature
298 ± 2 K
Ambient diffraction temperature
298 ± 2 K
Number of distinct elements
5
Space group number
14
Hermann-Mauguin space group symbol
P 1 21/c 1
Hall space group symbol
-P 2ybc
Residual factor for all reflections
0.0965
Residual factor for significantly intense reflections
0.0531
Weighted residual factors for significantly intense reflections
0.119
Weighted residual factors for all reflections included in the refinement
0.1343
Goodness-of-fit parameter for all reflections included in the refinement