Information card for entry 2015009

Structure parameters

• Chemical name: μ-Tri-tert-butylsilanethiolato-κ^2^S:S-bis[(tetrahydrofuran-κO)lithium(I)]
• Formula: C32 H70 Li2 O8 S2 Si2
• Calculated formula: C32 H70 Li2 O8 S2 Si2
• Title of publication: (μ-Tri-<i>tert</i>-butoxysilanethiolato)bis[(tetrahydrofuran)lithium(I)] and <i>catena</i>-poly[[bis(μ-tri-<i>tert</i>-butoxysilanethiolato)dilithium(I)]-μ-dimethoxyethane]: solvent coordination as the structure-forming factor
• Authors of publication: Elżbieta Jesionka; Anna Ciborska; Jaroslaw Chojnacki; Wieslaw Wojnowski
• Journal of publication: Acta Crystallographica Section C
• Year of publication: 2005
• Journal volume: 61
• Journal issue: 7
• Pages of publication: m321 - m323
• a: 9.789 ± 0.002 Å
• b: 20.083 ± 0.004 Å
• c: 11.746 ± 0.002 Å
• α: 90°
• β: 111.52 ± 0.03°
• γ: 90°
• Cell volume: 2148.2 ± 0.8 ų
• Cell temperature: 200 ± 2 K
• Ambient diffraction temperature: 200 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.1079
• Residual factor for significantly intense reflections: 0.0612
• Weighted residual factors for significantly intense reflections: 0.1952
• Weighted residual factors for all reflections included in the refinement: 0.2203
• Goodness-of-fit parameter for all reflections included in the refinement: 1.131
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: Yes