Information card for entry 2015133

Structure parameters

• Chemical name: Bis[(2-pyridyl)(2-pyridylamino)methanolato]cobalt(III) perchlorate
• Formula: C22 H20 Cl Co N6 O6
• Calculated formula: C22 H20 Cl Co N6 O6
• Title of publication: Bis[(2-pyridyl)(2-pyridylamino)methanolato]cobalt(III) perchlorate: a consequence of cobalt ion-assisted oxidative deamination of a tris(pyridyl)aminal ligand
• Authors of publication: Adams, Harry; Shongwe, Musa S.; Al-Bahri, Ibtisam; Al-Busaidi, Eiman; Morris, Michael J.
• Journal of publication: Acta Crystallographica Section C
• Year of publication: 2005
• Journal volume: 61
• Journal issue: 12
• Pages of publication: m497 - m500
• a: 14.802 ± 0.003 Å
• b: 8.6144 ± 0.0018 Å
• c: 17.832 ± 0.004 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 2273.8 ± 0.8 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 6
• Space group number: 29
• Hermann-Mauguin space group symbol: P c a 21
• Hall space group symbol: P 2c -2ac
• Residual factor for all reflections: 0.0668
• Residual factor for significantly intense reflections: 0.0599
• Weighted residual factors for significantly intense reflections: 0.1543
• Weighted residual factors for all reflections included in the refinement: 0.1593
• Goodness-of-fit parameter for all reflections included in the refinement: 1.119
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: Yes