Information card for entry 2015238

Structure parameters

• Chemical name: μ-oxalato-κ^2^O^1^,O^2^:κ^2^O^1'^,O^2'^-bis[(η^6^-p- cymene)(triphenylphosphine-κP)ruthenium(II)] bis(tetrafluoroborate)
• Formula: C58 H58 B2 F8 O4 P2 Ru2
• Calculated formula: C58 H58 B2 F8 O4 P2 Ru2
• Title of publication: Oxalate complexes of the (η^6^-<i>p</i>-cymene)ruthenium(II) fragment: μ-oxalato-κ^2^<i>O</i>^1^,<i>O</i>^2^:κ^2^<i>O</i>^1'^,<i>O</i>^2'^-bis[(η^6^-<i>p</i>-cymene)(triphenylphosphine-κ<i>P</i>)ruthenium(II)] bis(tetrafluoroborate) and (η^6^-<i>p</i>-cymene)(oxalato-κ^2^<i>O</i>,<i>O</i>')(pyridine-3,5-dicarboxylic acid-κ<i>N</i>)ruthenium(II)
• Authors of publication: Dale, Sophie H.; Elsegood, Mark R. J.
• Journal of publication: Acta Crystallographica Section C
• Year of publication: 2006
• Journal volume: 62
• Journal issue: 4
• Pages of publication: m166 - m170
• a: 9.4503 ± 0.0006 Å
• b: 16.8493 ± 0.001 Å
• c: 16.8539 ± 0.001 Å
• α: 90°
• β: 95.815 ± 0.002°
• γ: 90°
• Cell volume: 2669.9 ± 0.3 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.065
• Residual factor for significantly intense reflections: 0.0356
• Weighted residual factors for significantly intense reflections: 0.0684
• Weighted residual factors for all reflections included in the refinement: 0.0818
• Goodness-of-fit parameter for all reflections included in the refinement: 1.029
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: Yes