4-(2-Hydroxyphenyl)-2-phenyl-2,3-dihydro-1<i>H</i>-1,5-benzodiazepine and the 2-(2,3-dimethoxyphenyl)-, 2-(3,4-dimethoxyphenyl)- and 2-(2,5-dimethoxyphenyl)-substituted derivatives
Authors of publication
Escobar, Carlos A.; Donoso-Tauda, Oscar; Araya-Maturana, Ramiro; Vega, Andrés
Journal of publication
Acta Crystallographica Section C
Year of publication
2007
Journal volume
63
Journal issue
7
Pages of publication
o426 - o430
a
8.25 ± 0.002 Å
b
9.889 ± 0.003 Å
c
12.272 ± 0.003 Å
α
108.697 ± 0.004°
β
90.973 ± 0.005°
γ
90.594 ± 0.005°
Cell volume
948.1 ± 0.4 Å3
Cell temperature
298 ± 2 K
Ambient diffraction temperature
298 ± 2 K
Number of distinct elements
4
Space group number
2
Hermann-Mauguin space group symbol
P -1
Hall space group symbol
-P 1
Residual factor for all reflections
0.1319
Residual factor for significantly intense reflections
0.0619
Weighted residual factors for significantly intense reflections
0.144
Weighted residual factors for all reflections included in the refinement
0.1793
Goodness-of-fit parameter for all reflections included in the refinement