4-(2-Hydroxyphenyl)-2-phenyl-2,3-dihydro-1<i>H</i>-1,5-benzodiazepine and the 2-(2,3-dimethoxyphenyl)-, 2-(3,4-dimethoxyphenyl)- and 2-(2,5-dimethoxyphenyl)-substituted derivatives
Authors of publication
Escobar, Carlos A.; Donoso-Tauda, Oscar; Araya-Maturana, Ramiro; Vega, Andrés
Journal of publication
Acta Crystallographica Section C
Year of publication
2007
Journal volume
63
Journal issue
7
Pages of publication
o426 - o430
a
10.5071 ± 0.0003 Å
b
20.3901 ± 0.0006 Å
c
8.728 ± 0.0003 Å
α
90°
β
102.39 ± 0.002°
γ
90°
Cell volume
1826.34 ± 0.1 Å3
Cell temperature
296 ± 2 K
Ambient diffraction temperature
296 ± 2 K
Number of distinct elements
4
Space group number
14
Hermann-Mauguin space group symbol
P 1 21/c 1
Hall space group symbol
-P 2ybc
Residual factor for all reflections
0.0506
Residual factor for significantly intense reflections
0.0385
Weighted residual factors for significantly intense reflections
0.1108
Weighted residual factors for all reflections included in the refinement
0.1258
Goodness-of-fit parameter for all reflections included in the refinement