2,5-Dimethyl-6,7-dihydrobenzo[<i>h</i>]pyrazolo[1,5-<i>a</i>]quinazoline and 2-<i>tert</i>-butyl-5-methyl-6,7-dihydrobenzo[<i>h</i>]pyrazolo[1,5-<i>a</i>]quinazoline
Authors of publication
Portilla, Jaime; Quiroga, Jairo; Cobo, Justo; Low, John N.; Glidewell, Christopher
Journal of publication
Acta Crystallographica Section C
Year of publication
2007
Journal volume
63
Journal issue
8
Pages of publication
o458 - o461
a
11.2632 ± 0.0005 Å
b
11.4574 ± 0.0007 Å
c
12.1317 ± 0.0006 Å
α
93.449 ± 0.005°
β
90.313 ± 0.004°
γ
102.791 ± 0.006°
Cell volume
1523.66 ± 0.14 Å3
Cell temperature
120 ± 2 K
Ambient diffraction temperature
120 ± 2 K
Number of distinct elements
3
Space group number
2
Hermann-Mauguin space group symbol
P -1
Hall space group symbol
-P 1
Residual factor for all reflections
0.1255
Residual factor for significantly intense reflections
0.0649
Weighted residual factors for significantly intense reflections
0.1615
Weighted residual factors for all reflections included in the refinement
0.2129
Goodness-of-fit parameter for all reflections included in the refinement