Information card for entry 2016177

Structure parameters

• Chemical name: tetra-μ~2~-fluorido-tetradecafluoridotrizirconium(IV) hexahydrate
• Formula: Co2 F18 H46 N10 O8 Zr3
• Calculated formula: Co2 F18 H30 N10 O8 Zr3
• Title of publication: Double complexes [Co(NH~3~)~5~(H~2~O)]~2~[Zr~3~F~18~]·6H~2~O and [Co(NH~3~)~6~]~2~[Zr~3~F~18~]·6H~2~O
• Authors of publication: Gubanov, Alexander I.; Kuratieva, Natalia V.
• Journal of publication: Acta Crystallographica Section C
• Year of publication: 2007
• Journal volume: 63
• Journal issue: 10
• Pages of publication: i83 - i85
• a: 16.144 ± 0.0004 Å
• b: 12.7191 ± 0.0003 Å
• c: 14.6859 ± 0.0003 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 3015.56 ± 0.12 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 6
• Space group number: 72
• Hermann-Mauguin space group symbol: I b a m
• Hall space group symbol: -I 2 2c
• Residual factor for all reflections: 0.0515
• Residual factor for significantly intense reflections: 0.0473
• Weighted residual factors for significantly intense reflections: 0.107
• Weighted residual factors for all reflections included in the refinement: 0.1094
• Goodness-of-fit parameter for all reflections included in the refinement: 1.113
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: Yes