Information card for entry 2016215

Structure parameters

• Chemical name: Aqua-2κO-μ-{N,N'-bis[2-(dimethylamino)ethyl]oxamidato(2-)}- 1κ^2^O,O':2κ^4^N,N',N'',N'''-bis(4,4'-dimethyl-2,2'-bipyridine-1κ^2^N,N')- copper(II)nickel(II) bis(perchlorate) methanol hemisolvate
• Formula: C34.5 H40 Cl2 Cu N8 Ni O11.5
• Calculated formula: C34.5 H40 Cl2 Cu N8 Ni O11.5
• Title of publication: Aqua-2κ<i>O</i>-μ-{<i>N</i>,<i>N</i>'-bis[2-(dimethylamino)ethyl]oxamidato(2‒)}-1κ^2^<i>O</i>,<i>O</i>':2κ^4^<i>N</i>,<i>N</i>',<i>N</i>'',<i>N</i>'''-bis(4,4'-dimethyl-2,2'-bipyridine-1κ^2^<i>N</i>,<i>N</i>')copper(II)nickel(II) bis(perchlorate) methanol hemisolvate
• Authors of publication: Sun, Wei; Li, Yan-Tuan; Wu, Zhi-Yong; Liu, Jin-Liang
• Journal of publication: Acta Crystallographica Section C
• Year of publication: 2007
• Journal volume: 63
• Journal issue: 10
• Pages of publication: m462 - m464
• a: 21.347 ± 0.004 Å
• b: 14.852 ± 0.003 Å
• c: 25.087 ± 0.005 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 7954 ± 3 ų
• Cell temperature: 298 ± 2 K
• Ambient diffraction temperature: 298 ± 2 K
• Number of distinct elements: 7
• Space group number: 61
• Hermann-Mauguin space group symbol: P b c a
• Hall space group symbol: -P 2ac 2ab
• Residual factor for all reflections: 0.0991
• Residual factor for significantly intense reflections: 0.0503
• Weighted residual factors for significantly intense reflections: 0.1345
• Weighted residual factors for all reflections included in the refinement: 0.1855
• Goodness-of-fit parameter for all reflections included in the refinement: 1.105
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: Yes