Information card for entry 2016366

Structure parameters

• Chemical name: bis{μ-3-[2-(dimethylamino)ethylimino]butan-2-one oximato}dinickel(II) bis(perchlorate) acetonitrile solvate
• Formula: C18 H35 Cl2 N7 Ni2 O10
• Calculated formula: C18 H35 Cl2 N7 Ni2 O10
• Title of publication: Two new oximate-bridged square-planar dinuclear nickel(II) complexes
• Authors of publication: Bera, Manindranath; Noll, Bruce C.
• Journal of publication: Acta Crystallographica Section C
• Year of publication: 2007
• Journal volume: 63
• Journal issue: 12
• Pages of publication: m553 - m556
• a: 13.132 ± 0.0003 Å
• b: 12.2045 ± 0.0003 Å
• c: 17.2959 ± 0.0005 Å
• α: 90°
• β: 91.622 ± 0.0014°
• γ: 90°
• Cell volume: 2770.89 ± 0.12 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0437
• Residual factor for significantly intense reflections: 0.0349
• Weighted residual factors for significantly intense reflections: 0.0894
• Weighted residual factors for all reflections included in the refinement: 0.0948
• Goodness-of-fit parameter for all reflections included in the refinement: 1.056
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: Yes