Information card for entry 2016624

Structure parameters

• Common name: [(k2-N2-Bp)Mg(THF)(u-Cl)2Mg(THF)2(k2-N2-Bp)]
• Chemical name: di-μ-chlorido-bis[dihydridobis(pyrazol-1-yl)borato]- 1κ^2^<i>N</i>,<i>N</i>';2κ^2^<i>N</i>,<i>N</i>'-tris(tetrahydrofuran)- 1κ^2^O,2κO-dimagnesium(II)
• Formula: C24 H40 B2 Cl2 Mg2 N8 O3
• Calculated formula: C24 H40 B2 Cl2 Mg2 N8 O3
• Title of publication: Polymeric [dihydrobis(pyrazol-1-yl)borato]potassium(I) and three dihydrobis(pyrazol-1-yl)borate‒magnesium(I) compounds obtained by disproportionation of the Grignard reagent
• Authors of publication: Loroño-Gonzalez, D. J.
• Journal of publication: Acta Crystallographica Section C
• Year of publication: 2008
• Journal volume: 64
• Journal issue: 6
• Pages of publication: m228 - m232
• a: 15.119 ± 0.003 Å
• b: 13.862 ± 0.002 Å
• c: 15.453 ± 0.003 Å
• α: 90°
• β: 99.319 ± 0.003°
• γ: 90°
• Cell volume: 3195.9 ± 1 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0682
• Residual factor for significantly intense reflections: 0.0542
• Weighted residual factors for significantly intense reflections: 0.1257
• Weighted residual factors for all reflections included in the refinement: 0.1331
• Goodness-of-fit parameter for all reflections included in the refinement: 1.079
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: Yes