Information card for entry 2016684

Structure parameters

• Chemical name: (2,2'-diazenediyldiphenolato-κ^3^<i>O</i>,<i>N</i>,<i>O</i>')dimethylsilicon
• Formula: C14 H14 N2 O2 Si
• Calculated formula: C14 H14 N2 O2 Si
• Title of publication: Dynamic disorder in a pentacoordinate silicon complex with 2,2'-diazenediyldiphenol
• Authors of publication: Böhme, Uwe; Jähnigen, Sandra
• Journal of publication: Acta Crystallographica Section C
• Year of publication: 2008
• Journal volume: 64
• Journal issue: 7
• Pages of publication: o364 - o366
• a: 10.2295 ± 0.0002 Å
• b: 8.0212 ± 0.0001 Å
• c: 32.1141 ± 0.0005 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 2635.05 ± 0.07 ų
• Cell temperature: 298 ± 2 K
• Ambient diffraction temperature: 298 ± 2 K
• Number of distinct elements: 5
• Space group number: 61
• Hermann-Mauguin space group symbol: P b c a
• Hall space group symbol: -P 2ac 2ab
• Residual factor for all reflections: 0.0621
• Residual factor for significantly intense reflections: 0.0458
• Weighted residual factors for significantly intense reflections: 0.1276
• Weighted residual factors for all reflections included in the refinement: 0.1436
• Goodness-of-fit parameter for all reflections included in the refinement: 1.108
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: Yes