Four <i>N</i>^7^-alkoxybenzyl-substituted 4,5,6,7-tetrahydro-1<i>H</i>-pyrazolo[3,4-<i>b</i>]pyridine-5-spiro-1'-cyclohexane-2',6'-diones: hydrogen-bonded supramolecular structures in zero, one, two or three dimensions
Authors of publication
Trilleras, Jorge; Quiroga, Jairo; Cobo, Justo; Low, John N.; Glidewell, Christopher
Journal of publication
Acta Crystallographica Section C
Year of publication
2008
Journal volume
64
Journal issue
12
Pages of publication
o665 - o670
a
9.2691 ± 0.0014 Å
b
11.0898 ± 0.0011 Å
c
12.802 ± 0.002 Å
α
92.844 ± 0.01°
β
95.185 ± 0.012°
γ
91.07 ± 0.011°
Cell volume
1308.6 ± 0.3 Å3
Cell temperature
120 ± 2 K
Ambient diffraction temperature
120 ± 2 K
Number of distinct elements
4
Space group number
2
Hermann-Mauguin space group symbol
P -1
Hall space group symbol
-P 1
Residual factor for all reflections
0.1695
Residual factor for significantly intense reflections
0.0626
Weighted residual factors for significantly intense reflections
0.1289
Weighted residual factors for all reflections included in the refinement
0.1712
Goodness-of-fit parameter for all reflections included in the refinement