Information card for entry 2017019

Structure parameters

• Chemical name: bis[μ~3~-<i>cis</i>-<i>N</i>-(2-aminopropyl)-<i>N</i>'-(2- carboxylatophenyl)oxamidato(3-)]-1:2:4κ^7^<i>N</i>,<i>N</i>',<i>N</i>'', <i>O</i>:<i>O</i>',<i>O</i>":<i>O</i>''';2:4:3κ^7^<i>O</i>''':<i>O</i>', <i>O</i>":<i>N</i>,<i>N</i>',<i>N</i>'',<i>O</i>-bis(2,2'-bipyridine)- 2κ^2^<i>N</i>,<i>N</i>';4κ^2^<i>N</i>,<i>N</i>'-dichlorido-1κCl,3κCl- tetracopper(II) dihydrate
• Formula: C44 H44 Cl2 Cu4 N10 O10
• Calculated formula: C44 H44 Cl2 Cu4 N10 O10
• Title of publication: Bis[μ~3~-<i>cis</i>-<i>N</i>-(2-aminopropyl)-<i>N</i>'-(2-carboxylatophenyl)oxamidato(3‒)]bis(2,2'-bipyridine)dichloridotetracopper(II) dihydrate
• Authors of publication: Gu, Yuan-Yuan; Li, Yan-Tuan; Wu, Zhi-Yong; Sun, Wei; Jiang, Man
• Journal of publication: Acta Crystallographica Section C
• Year of publication: 2009
• Journal volume: 65
• Journal issue: 3
• Pages of publication: m115 - m117
• a: 10.9622 ± 0.0001 Å
• b: 11.133 ± 0.0002 Å
• c: 11.2876 ± 0.0002 Å
• α: 67.072 ± 0.001°
• β: 69.842 ± 0.001°
• γ: 72.688 ± 0.001°
• Cell volume: 1169.57 ± 0.03 ų
• Cell temperature: 298 ± 2 K
• Ambient diffraction temperature: 298 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0498
• Residual factor for significantly intense reflections: 0.0354
• Weighted residual factors for significantly intense reflections: 0.0884
• Weighted residual factors for all reflections included in the refinement: 0.0982
• Goodness-of-fit parameter for all reflections included in the refinement: 1.042
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: Yes