(2<i>R</i>,4<i>S</i>)-7-Bromo-2-phenyl-2,3,4,5-tetrahydro-1,4-epoxynaphtho[1,2-<i>b</i>]azepine, (2<i>RS</i>,4<i>SR</i>)-7-bromo-2-(4-chlorophenyl-2,3,4,5-tetrahydro-1,4-epoxynaphtho[1,2-<i>b</i>]azepine and (2<i>RS</i>,4<i>SR</i>)-2-(4-fluorophenyl)-2,3,4,5-tetrahydro-1,4-epoxynaphtho[1,2-<i>b</i>]azepine: hydrogen-bonded structures in two and three dimensions
Authors of publication
Palma, Alirio; Bahsas, Ali; Yépes, Andrés F.; Cobo, Justo; Hursthouse, Michael B.; Glidewell, Christopher
Journal of publication
Acta Crystallographica Section C
Year of publication
2009
Journal volume
65
Journal issue
4
Pages of publication
o140 - o145
a
7.8444 ± 0.0003 Å
b
9.8146 ± 0.0004 Å
c
10.0871 ± 0.0004 Å
α
90°
β
92.103 ± 0.003°
γ
90°
Cell volume
776.08 ± 0.05 Å3
Cell temperature
120 ± 2 K
Ambient diffraction temperature
120 ± 2 K
Number of distinct elements
5
Space group number
4
Hermann-Mauguin space group symbol
P 1 21 1
Hall space group symbol
P 2yb
Residual factor for all reflections
0.0577
Residual factor for significantly intense reflections
0.046
Weighted residual factors for significantly intense reflections
0.0951
Weighted residual factors for all reflections included in the refinement
0.1019
Goodness-of-fit parameter for all reflections included in the refinement