5-(4,5-Ethylenedithio-1,3-dithiol-2-ylidene)-1,3,4,6-tetrathiapentalen-2-one (EDTO‒TTP) and 5-[4,5-(ethene-1,2-diyldithio)-1,3-dithiol-2-ylidene]-1,3,4,6-tetrathiapentalen-2-one (VDTO‒TTP)
Authors of publication
Chen, Hong-Feng; Fang, Qi; Yu, Wen-Tao; Batsanov, Andrei S.; Howard, Judith A. K.
Journal of publication
Acta Crystallographica Section C
Year of publication
2009
Journal volume
65
Journal issue
5
Pages of publication
o198 - o201
a
6.4948 ± 0.0004 Å
b
28.7194 ± 0.0016 Å
c
7.1503 ± 0.0004 Å
α
90°
β
99.548 ± 0.001°
γ
90°
Cell volume
1315.25 ± 0.13 Å3
Cell temperature
220 ± 2 K
Ambient diffraction temperature
220 ± 2 K
Number of distinct elements
4
Space group number
14
Hermann-Mauguin space group symbol
P 1 21/n 1
Hall space group symbol
-P 2yn
Residual factor for all reflections
0.0431
Residual factor for significantly intense reflections
0.0289
Weighted residual factors for significantly intense reflections
0.0593
Weighted residual factors for all reflections included in the refinement
0.0643
Goodness-of-fit parameter for all reflections included in the refinement