Eight 7-benzyl-3-<i>tert</i>-butyl-1-phenylpyrazolo[3,4-<i>d</i>]oxazines, encompassing structures containing no intermolecular hydrogen bonds, and hydrogen-bonded structures in one, two or three dimensions
Authors of publication
Castillo, Juan C.; Abonía, Rodrigo; Cobo, Justo; Glidewell, Christopher
Journal of publication
Acta Crystallographica Section C
Year of publication
2009
Journal volume
65
Journal issue
8
Pages of publication
o423 - o430
a
8.893 ± 0.001 Å
b
11.1321 ± 0.0012 Å
c
10.2078 ± 0.0009 Å
α
90°
β
109.749 ± 0.007°
γ
90°
Cell volume
951.11 ± 0.18 Å3
Cell temperature
120 ± 2 K
Ambient diffraction temperature
120 ± 2 K
Number of distinct elements
4
Space group number
4
Hermann-Mauguin space group symbol
P 1 21 1
Hall space group symbol
P 2yb
Residual factor for all reflections
0.0718
Residual factor for significantly intense reflections
0.0434
Weighted residual factors for significantly intense reflections
0.0891
Weighted residual factors for all reflections included in the refinement
0.1027
Goodness-of-fit parameter for all reflections included in the refinement