Di-μ-oxido-bis{bis[<i>N</i>,<i>N</i>'-bis(2-pyridylmethyl)ethane-1,2-diamine]manganese(III,IV)} tris(perchlorate) hexahydrate: clarification of an order‒disorder phase transition
Authors of publication
Nielsen, Anne; McKenzie, Christine J.; Bond, Andrew D.
Journal of publication
Acta Crystallographica Section C
Year of publication
2009
Journal volume
65
Journal issue
11
Pages of publication
m447 - m450
a
15.4488 ± 0.0007 Å
b
12.2792 ± 0.0005 Å
c
23.7512 ± 0.001 Å
α
90°
β
106.852 ± 0.002°
γ
90°
Cell volume
4312.1 ± 0.3 Å3
Cell temperature
295 ± 2 K
Ambient diffraction temperature
295 ± 2 K
Number of distinct elements
6
Space group number
15
Hermann-Mauguin space group symbol
C 1 2/c 1
Hall space group symbol
-C 2yc
Residual factor for all reflections
0.0866
Residual factor for significantly intense reflections
0.0672
Weighted residual factors for significantly intense reflections
0.2196
Weighted residual factors for all reflections included in the refinement
0.2347
Goodness-of-fit parameter for all reflections included in the refinement