Monitoring structural transformations in crystals. 13. On photocyclization in 2,3,4,5,6-pentamethylbenzophenone, 1,3-diphenylbutan-1-one and 2,4,6-triisopropyl-4'-methoxybenzophenone
Authors of publication
Bakowicz, Julia; Turowska-Tyrk, Ilona
Journal of publication
Acta Crystallographica Section C
Year of publication
2010
Journal volume
66
Journal issue
1
Pages of publication
o29 - o32
a
10.7926 ± 0.0018 Å
b
14.931 ± 0.002 Å
c
7.8275 ± 0.0011 Å
α
90°
β
90°
γ
90°
Cell volume
1261.4 ± 0.3 Å3
Cell temperature
299 ± 2 K
Ambient diffraction temperature
299 ± 2 K
Number of distinct elements
3
Space group number
29
Hermann-Mauguin space group symbol
P c a 21
Hall space group symbol
P 2c -2ac
Residual factor for all reflections
0.0438
Residual factor for significantly intense reflections
0.0382
Weighted residual factors for significantly intense reflections
0.1088
Weighted residual factors for all reflections included in the refinement
0.1152
Goodness-of-fit parameter for all reflections included in the refinement