Information card for entry 2017753

Structure parameters

• Chemical name: 5,10,15,20-tetrakis(pyridin-1-ium-4-yl)porphyrin pentaaquadinitratodysprosate(III) pentanitrate diethanol solvate dihydrate
• Formula: C44 H56 Dy N15 O30
• Calculated formula: C44 H56 Dy N15 O30
• Title of publication: Coordination and hydrogen-bonding assemblies in hybrid reaction products between 5,10,15,20-tetra-4-pyridylporphyrin and dysprosium trinitrate hexahydrate
• Authors of publication: Lipstman, Sophia; Goldberg, Israel
• Journal of publication: Acta Crystallographica Section C
• Year of publication: 2010
• Journal volume: 66
• Journal issue: 8
• Pages of publication: m222 - m226
• a: 12.8961 ± 0.0002 Å
• b: 12.9222 ± 0.0002 Å
• c: 18.5978 ± 0.0003 Å
• α: 71.6843 ± 0.0007°
• β: 80.9684 ± 0.0008°
• γ: 73.3707 ± 0.0007°
• Cell volume: 2811.52 ± 0.08 ų
• Cell temperature: 110 ± 2 K
• Ambient diffraction temperature: 110 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0404
• Residual factor for significantly intense reflections: 0.0335
• Weighted residual factors for significantly intense reflections: 0.0784
• Weighted residual factors for all reflections included in the refinement: 0.0817
• Goodness-of-fit parameter for all reflections included in the refinement: 1.043
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: Yes