Cyclic imides and an open-chain amide carboxylic acid from the facile reaction of <i>cis</i>-cyclohexane-1,2-carboxylic anhydride with the isomeric monofluoroanilines
Authors of publication
Smith, Graham; Wermuth, Urs D.
Journal of publication
Acta Crystallographica Section C
Year of publication
2012
Journal volume
68
Journal issue
7
Pages of publication
o253 - o256
a
8.0316 ± 0.0004 Å
b
8.1702 ± 0.0004 Å
c
9.2085 ± 0.0005 Å
α
98.595 ± 0.004°
β
93.324 ± 0.004°
γ
97.26 ± 0.004°
Cell volume
590.86 ± 0.05 Å3
Cell temperature
200 ± 2 K
Ambient diffraction temperature
200 ± 2 K
Number of distinct elements
5
Space group number
2
Hermann-Mauguin space group symbol
P -1
Hall space group symbol
-P 1
Residual factor for all reflections
0.0494
Residual factor for significantly intense reflections
0.0354
Weighted residual factors for significantly intense reflections
0.0939
Weighted residual factors for all reflections included in the refinement
0.0979
Goodness-of-fit parameter for all reflections included in the refinement