Information card for entry 2018926

Structure parameters

• Chemical name: Tetrakis[μ~3~-(pyridin-2-yl)methanolato]-<i>tetrahedro</i>-tetrakis[chloridolead(II)]
• Formula: C24 H24 Cl4 N4 O4 Pb4
• Calculated formula: C24 H24 Cl4 N4 O4 Pb4
• SMILES: [O]12([Pb]3(Cl)[O]4(Cc5ccccn5)[Pb]1(Cl)[O]1(Cc5ccccn5)[Pb]2([O]3(Cc2ccccn2)[Pb]41Cl)Cl)Cc1ccccn1
• Title of publication: Two novel lead(II) complexes of 2-(hydroxymethyl)pyridine: a threefold diamondoid supramolecular network based on Pb~4~O~4~ cores and a two-dimensional (4,4) network based on Pb~2~O~2~ units
• Authors of publication: Liu, Ting; Pan, Yu-Peng; Wang, Suna; Dou, Jian-Min
• Journal of publication: Acta Crystallographica Section C
• Year of publication: 2013
• Journal volume: 69
• Journal issue: 4
• Pages of publication: 394 - 399
• a: 15.373 ± 0.003 Å
• b: 15.373 ± 0.003 Å
• c: 13.287 ± 0.002 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 3140.1 ± 1 ų
• Cell temperature: 298 ± 2 K
• Ambient diffraction temperature: 298 ± 2 K
• Number of distinct elements: 6
• Space group number: 88
• Hermann-Mauguin space group symbol: I 41/a :2
• Hall space group symbol: -I 4ad
• Residual factor for all reflections: 0.0375
• Residual factor for significantly intense reflections: 0.026
• Weighted residual factors for significantly intense reflections: 0.0572
• Weighted residual factors for all reflections included in the refinement: 0.0609
• Goodness-of-fit parameter for all reflections included in the refinement: 1.14
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: Yes