Information card for entry 2019011

Structure parameters

• Chemical name: Tetrakis(tetrahydrofuran)lithium tetrakis[(trimethylsilyl)methyl]borate
• Formula: C32 H76 B Li O4 Si4
• Calculated formula: C32 H76 B Li O4 Si4
• Title of publication: An approach to creating novel anions: silylated triel compounds with ‒CH~2~‒ and ‒O‒ linkers, [InCl~2~{O(HO)Si(<i>t</i>-Bu)~2~}]~2~ and Li[B(CH~2~SiMe~3~)~4~]
• Authors of publication: Scholz, Stefan; Vitze, Hannes; Bolte, Michael; Lerner, Hans-Wolfram
• Journal of publication: Acta Crystallographica Section C
• Year of publication: 2013
• Journal volume: 69
• Journal issue: 6
• Pages of publication: 569 - 572
• a: 10.5661 ± 0.0007 Å
• b: 11.7334 ± 0.001 Å
• c: 18.1342 ± 0.0012 Å
• α: 90°
• β: 93.153 ± 0.005°
• γ: 90°
• Cell volume: 2244.8 ± 0.3 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 6
• Space group number: 7
• Hermann-Mauguin space group symbol: P 1 n 1
• Hall space group symbol: P -2yac
• Residual factor for all reflections: 0.1299
• Residual factor for significantly intense reflections: 0.0706
• Weighted residual factors for significantly intense reflections: 0.1163
• Weighted residual factors for all reflections included in the refinement: 0.1354
• Goodness-of-fit parameter for all reflections included in the refinement: 0.96
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: Yes