Information card for entry 2019035
Chemical name |
<i>cis</i>-Dichlorido(3,6,9-trithiabicyclo[9.3.1]pentadecane-κ^2^<i>S</i>^3^,<i>S</i>^6^)palladium(II) acetonitrile 0.8-solvate |
Formula |
C13.6 H24.4 Cl2 N0.8 Pd S3 |
Calculated formula |
C13.588 H24.382 Cl2 N0.794 Pd S3 |
Title of publication |
<i>cis</i>-Dichlorido(3,6,9-trithiabicyclo[9.3.1]pentadecane-κ^2^<i>S</i>^3^,<i>S</i>^6^)palladium(II) acetonitrile 0.8-solvate |
Authors of publication |
Dawe, Louise Nicole; Penney, Lisa; Black, Daniel A.; Miller, David O.; Lucas, C. Robert |
Journal of publication |
Acta Crystallographica Section C |
Year of publication |
2013 |
Journal volume |
69 |
Journal issue |
7 |
Pages of publication |
727 - 729 |
a |
24.906 ± 0.004 Å |
b |
18.144 ± 0.002 Å |
c |
8.328 ± 0.002 Å |
α |
90° |
β |
90° |
γ |
90° |
Cell volume |
3763.4 ± 1.2 Å3 |
Cell temperature |
299 ± 2 K |
Ambient diffraction temperature |
299 ± 2 K |
Number of distinct elements |
6 |
Space group number |
61 |
Hermann-Mauguin space group symbol |
P b c a |
Hall space group symbol |
-P 2ac 2ab |
Residual factor for all reflections |
0.0992 |
Residual factor for significantly intense reflections |
0.0376 |
Weighted residual factors for significantly intense reflections |
0.0926 |
Weighted residual factors for all reflections included in the refinement |
0.1093 |
Goodness-of-fit parameter for all reflections included in the refinement |
0.99 |
Diffraction radiation wavelength |
0.71069 Å |
Diffraction radiation type |
MoKα |
Has coordinates |
Yes |
Has disorder |
Yes |
Has Fobs |
Yes |
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