Information card for entry 2019262

Structure parameters

• Chemical name: Chlorido{μ-2-[(2-oxidobenzylidene)amino]ethan-1-olato-κ^4^<i>O</i>,<i>N</i>,<i>O</i>':<i>O</i>'}{2-[(2-oxidobenzylidene)amino]ethan-1-olato-κ^3^<i>O</i>,<i>N</i>,<i>O</i>'}trivinylditin(IV)
• Formula: C24 H27 Cl N2 O4 Sn2
• Calculated formula: C24 H27 Cl N2 O4 Sn2
• SMILES: [Sn]12([O]([Sn]34(Cl)(OCC[N]4=Cc4c(O3)cccc4)C=C)CC[N]2=Cc2c(O1)cccc2)(C=C)C=C
• Title of publication: Enantiotropic phase transition in a binuclear tin complex with an <i>O</i>,<i>N</i>,<i>O</i>'-tridentate ligand
• Authors of publication: Schwarzer, Anke; Paul, Lydia E. H.; Böhme, Uwe
• Journal of publication: Acta Crystallographica Section C
• Year of publication: 2013
• Journal volume: 69
• Journal issue: 11
• Pages of publication: 1336 - 1339
• a: 13.2848 ± 0.0003 Å
• b: 15.7966 ± 0.0004 Å
• c: 25.7287 ± 0.0006 Å
• α: 90°
• β: 109.176 ± 0.001°
• γ: 90°
• Cell volume: 5099.7 ± 0.2 ų
• Cell temperature: 93 ± 2 K
• Ambient diffraction temperature: 93 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0479
• Residual factor for significantly intense reflections: 0.0327
• Weighted residual factors for significantly intense reflections: 0.0611
• Weighted residual factors for all reflections included in the refinement: 0.0658
• Goodness-of-fit parameter for all reflections included in the refinement: 1.091
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No