Information card for entry 2019710

Structure parameters

• Chemical name: Poly[piperazine-1,4-dium [tetra-μ~3~-azido-κ^12^<i>N</i>^1^:<i>N</i>^1^:<i>N</i>^1^-hexa-μ~2~-azido-κ^12^<i>N</i>^1^:<i>N</i>^1^-di-μ~2~-azido-κ^4^<i>N</i>^1^:<i>N</i>^3^-pentacopper(II)] tetrahydrate]
• Formula: C4 H20 Cu5 N38 O4
• Calculated formula: C4 H20 Cu5 N38 O4
• Title of publication: An azide-bridged copper(II) complex: poly[piperazine-1,4-dium [tetra-μ~3~-azido-κ^12^<i>N</i>^1^:<i>N</i>^1^:<i>N</i>^1^-hexa-μ~2~-azido-κ^12^<i>N</i>^1^:<i>N</i>^1^-di-μ~2~-azido-κ^4^<i>N</i>^1^:<i>N</i>^3^-pentacopper(II)] tetrahydrate]
• Authors of publication: Liu, Hou-Ting; Lu, Jing
• Journal of publication: Acta Crystallographica Section C
• Year of publication: 2014
• Journal volume: 70
• Journal issue: 11
• Pages of publication: 1083 - 1087
• a: 16.343 ± 0.003 Å
• b: 5.7477 ± 0.0011 Å
• c: 16.812 ± 0.003 Å
• α: 90°
• β: 91.1 ± 0.03°
• γ: 90°
• Cell volume: 1578.9 ± 0.5 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0506
• Residual factor for significantly intense reflections: 0.0314
• Weighted residual factors for significantly intense reflections: 0.0634
• Weighted residual factors for all reflections included in the refinement: 0.0724
• Goodness-of-fit parameter for all reflections included in the refinement: 1.02
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: Yes