Synthesis and crystal structure of 2-amino-3-hydroxypyridinium dioxido(pyridine-2,6-dicarboxylato-κ^3^<i>O</i>^2^,<i>N</i>,<i>O</i>^6^)vanadate(V) and its conversion to nanostructured V~2~O~5~
Authors of publication
Hejrani-Dalir, Ali; Tabatabaee, Masumeh; Sheibani, Ali
Journal of publication
Acta Crystallographica Section C
Year of publication
2015
Journal volume
71
Journal issue
2
a
26.173 ± 0.003 Å
b
6.3586 ± 0.0007 Å
c
8.1089 ± 0.0008 Å
α
90°
β
90°
γ
90°
Cell volume
1349.5 ± 0.3 Å3
Cell temperature
147 ± 2 K
Ambient diffraction temperature
147 ± 2 K
Number of distinct elements
5
Space group number
62
Hermann-Mauguin space group symbol
P n m a
Hall space group symbol
-P 2ac 2n
Residual factor for all reflections
0.0374
Residual factor for significantly intense reflections
0.0347
Weighted residual factors for significantly intense reflections
0.082
Weighted residual factors for all reflections included in the refinement
0.0832
Goodness-of-fit parameter for all reflections included in the refinement