Information card for entry 2019823

Structure parameters

• Chemical name: Tricarbonyl(μ-diphenylphosphido-κ^2^<i>P</i>:<i>P</i>)(methyldiphenylsilyl-κ<i>Si</i>)bis(triphenylphosphane-κ<i>P</i>)iron(II)platinum(0)(<i>Fe</i>—<i>Pt</i>) dichloromethane hemisolvate
• Formula: C64.5 H54 Cl Fe O3 P3 Pt Si
• Calculated formula: C64.5 H54 Cl Fe O3 P3 Pt Si
• Title of publication: Crystal structure of tricarbonyl(μ-diphenylphosphido-κ2P:P)(methyldiphenylsilyl-κSi)bis(triphenylphosphane-κP)iron(II)platinum(0)(Fe—Pt)
• Authors of publication: Mohamed, Ahmed Said; Jourdain, Isabelle; Knorr, Michael; Rousselin, Yoann; Kubicki, Marek M.
• Journal of publication: Acta Crystallographica Section E Crystallographic Communications
• Year of publication: 2015
• Journal volume: 71
• Journal issue: 2
• Pages of publication: 241
• a: 10.3522 ± 0.0006 Å
• b: 13.001 ± 0.0008 Å
• c: 21.9803 ± 0.0014 Å
• α: 99.823 ± 0.002°
• β: 99.061 ± 0.002°
• γ: 102.677 ± 0.002°
• Cell volume: 2784.8 ± 0.3 ų
• Cell temperature: 115 K
• Ambient diffraction temperature: 115 K
• Number of distinct elements: 8
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.037
• Residual factor for significantly intense reflections: 0.0271
• Weighted residual factors for significantly intense reflections: 0.0595
• Weighted residual factors for all reflections included in the refinement: 0.0626
• Goodness-of-fit parameter for all reflections included in the refinement: 1.055
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: Yes