Information card for entry 2019866

Structure parameters

• Chemical name: Tris(tri-<i>o</i>-tolylphosphite-κ<i>P</i>)nickel(II)
• Formula: C63 H63 Ni O9 P3
• Calculated formula: C63 H63 Ni O9 P3
• Title of publication: Tris(tri-<i>o</i>-tolyl phosphite-κ<i>P</i>)nickel: a coordinatively unsaturated nickel(0) complex
• Authors of publication: Kampmann, Sven S.; Skelton, Brian W.; Wild, Duncan A.; Koutsantonis, George A.; Stewart, Scott G.
• Journal of publication: Acta Crystallographica Section C
• Year of publication: 2015
• Journal volume: 71
• Journal issue: 3
• a: 21.5898 ± 0.0009 Å
• b: 12.3292 ± 0.0003 Å
• c: 43.403 ± 0.002 Å
• α: 90°
• β: 104.129 ± 0.005°
• γ: 90°
• Cell volume: 11203.7 ± 0.8 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 5
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.1144
• Residual factor for significantly intense reflections: 0.0994
• Weighted residual factors for significantly intense reflections: 0.2454
• Weighted residual factors for all reflections included in the refinement: 0.2586
• Goodness-of-fit parameter for all reflections included in the refinement: 1.057
• Diffraction radiation wavelength: 1.54178 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: Yes