Unusual centrosymmetric structure of [<i>M</i>(18-crown-6)]^+^ (<i>M</i> = Rb, Cs and NH~4~) complexes stabilized in an environment of hexachloridoantimonate(V) anions
Authors of publication
Ponomarova, Vira V.; Rusanova, Julia A.; Rusanov, Eduard B.; Domasevitch, Konstantin V.
Journal of publication
Acta Crystallographica Section C
Year of publication
2015
Journal volume
71
Journal issue
10
a
14.1069 ± 0.0009 Å
b
14.1069 ± 0.0009 Å
c
10.1908 ± 0.0008 Å
α
90°
β
90°
γ
120°
Cell volume
1756.3 ± 0.2 Å3
Cell temperature
223 ± 2 K
Ambient diffraction temperature
223 ± 2 K
Number of distinct elements
6
Space group number
148
Hermann-Mauguin space group symbol
R -3 :H
Hall space group symbol
-R 3
Residual factor for all reflections
0.0236
Residual factor for significantly intense reflections
0.0217
Weighted residual factors for significantly intense reflections
0.0547
Weighted residual factors for all reflections included in the refinement
0.0556
Goodness-of-fit parameter for all reflections included in the refinement