A synchrotron study of [5,10,15,20-tetrakis(3-cyanophenyl)porphyrinato-κ^4^<i>N</i>^5^,<i>N</i>^10^,<i>N</i>^15^,<i>N</i>^20^]copper(II) nitrobenzene trisolvate at 80K
Authors of publication
Seidel, Rüdiger W.; Goddard, Richard; Mayer-Gall, Thomas; Oppel, Iris M.
Journal of publication
Acta Crystallographica Section C
Year of publication
2016
Journal volume
72
Journal issue
11
Pages of publication
861 - 866
a
8.234 ± 0.004 Å
b
11.872 ± 0.009 Å
c
14.212 ± 0.007 Å
α
104.37 ± 0.03°
β
94.85 ± 0.1°
γ
96.85 ± 0.08°
Cell volume
1326.8 ± 1.4 Å3
Cell temperature
80 ± 2 K
Ambient diffraction temperature
80 ± 2 K
Number of distinct elements
5
Space group number
2
Hermann-Mauguin space group symbol
P -1
Hall space group symbol
-P 1
Residual factor for all reflections
0.0529
Residual factor for significantly intense reflections
0.049
Weighted residual factors for significantly intense reflections
0.1273
Weighted residual factors for all reflections included in the refinement
0.1297
Goodness-of-fit parameter for all reflections included in the refinement
