Information card for entry 2021403

Structure parameters

• Chemical name: Ytterbium octapotassiumdisodium triaquacarbonato(germanotungstato)triyttrium hexadecahydrate
• Formula: C Ge2 K8 Na O93 W18 Yb4
• Calculated formula: C Ge2 K8 Na O93 W18 Yb4
• Title of publication: Synthesis and characterization of carbonate-encapsulated ytterbium- and yttrium-containing polyoxotungstates
• Authors of publication: Kaushik, Reetam; Khan, Imran; Saini, Mukesh Kumar; Hussain, Firasat; Sadakane, Masahiro
• Journal of publication: Acta Crystallographica Section C
• Year of publication: 2018
• Journal volume: 74
• Journal issue: 11
• Pages of publication: 1355 - 1361
• a: 22.2367 ± 0.0006 Å
• b: 22.6726 ± 0.0005 Å
• c: 20.1786 ± 0.0005 Å
• α: 90°
• β: 111.037 ± 0.003°
• γ: 90°
• Cell volume: 9495.3 ± 0.4 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 7
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0551
• Residual factor for significantly intense reflections: 0.0432
• Weighted residual factors for significantly intense reflections: 0.1049
• Weighted residual factors for all reflections included in the refinement: 0.111
• Goodness-of-fit parameter for all reflections included in the refinement: 1.038
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No