Information card for entry 2022431

Structure parameters

• Chemical name: Bis[μ-<i>N</i>,<i>N</i>'-bis(2,6-diisopropylphenyl)formamidinato]diantimony(I)(2 <i>Sb</i>—<i>Sb</i>) tetrahydrofuran heptasolvate
• Formula: C78 H126 N4 O7 Sb2
• Calculated formula: C78 H126 N4 O7 Sb2
• Title of publication: Synthesis and characterization of a range of antimony(I/III) <i>N</i>,<i>N</i>'-bis(2,6-diisopropylphenyl)formamidinate complexes
• Authors of publication: Al-Dabbagh, Areej; Guo, Zhifang; Junk, Peter; Wang, Jun
• Journal of publication: Acta Crystallographica Section C
• Year of publication: 2021
• Journal volume: 77
• Journal issue: 9
• a: 21.243 ± 0.004 Å
• b: 18.997 ± 0.004 Å
• c: 21.743 ± 0.004 Å
• α: 90°
• β: 118.6 ± 0.03°
• γ: 90°
• Cell volume: 7704 ± 3 ų
• Cell temperature: 100 K
• Ambient diffraction temperature: 100 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.1045
• Residual factor for significantly intense reflections: 0.0914
• Weighted residual factors for significantly intense reflections: 0.2653
• Weighted residual factors for all reflections included in the refinement: 0.2713
• Goodness-of-fit parameter for all reflections included in the refinement: 1.188
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: Synchrotron
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: Yes