Information card for entry 2022535

Structure parameters

• Chemical name: <i>catena</i>-Poly[bis(μ-~3~η^4^:η^6^:η^4^-naphthalene)tetrakis(tetrahydrofuran)dipotassiumvanadium]
• Formula: C36 H48 K2 O4 V
• Calculated formula: C36 H48 K2 O4 V
• Title of publication: Syntheses and crystal structures of new naphthalene– and anthracene–vanadate salts and an unprecedented dimetallabis(anthracene) sandwich complex: [Na(tetrahydrofuran)~3~][V~2~(anthracene)~2~]
• Authors of publication: Kucera, Benjamin E.; Young, Jr, Victor G.; Brennessel, William W.; Ellis, John E.
• Journal of publication: Acta Crystallographica Section C
• Year of publication: 2022
• Journal volume: 78
• Journal issue: 3
• a: 10.985 ± 0.002 Å
• b: 17.243 ± 0.004 Å
• c: 18.532 ± 0.004 Å
• α: 90°
• β: 101.014 ± 0.003°
• γ: 90°
• Cell volume: 3445.6 ± 1.3 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0858
• Residual factor for significantly intense reflections: 0.0474
• Weighted residual factors for significantly intense reflections: 0.1061
• Weighted residual factors for all reflections included in the refinement: 0.12
• Goodness-of-fit parameter for all reflections included in the refinement: 1.024
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: Yes