Information card for entry 2022537

Structure parameters

• Chemical name: (1,4,7,10,13,16-Hexaoxacyclooctadecane)bis(tetrahydrofuran)potassium [(η^4^-anthracene)(tetrahydrofuran)vanadium]-μ-η^4^:η^2^-anthracene-[(1,4,7,10,13,16-Hexaoxacyclooctadecane)potassium]-μ-η^2^:η^4^-anthracene-[(η^4^-anthracene)(tetrahydrofuran)vanadium] tetrahydrofuran disolvate
• Formula: C104 H136 K2 O18 V2
• Calculated formula: C104 H136 K2 O18 V2
• Title of publication: Syntheses and crystal structures of new naphthalene– and anthracene–vanadate salts and an unprecedented dimetallabis(anthracene) sandwich complex: [Na(tetrahydrofuran)~3~][V~2~(anthracene)~2~]
• Authors of publication: Kucera, Benjamin E.; Young, Jr, Victor G.; Brennessel, William W.; Ellis, John E.
• Journal of publication: Acta Crystallographica Section C
• Year of publication: 2022
• Journal volume: 78
• Journal issue: 3
• a: 9.1729 ± 0.0016 Å
• b: 9.3501 ± 0.0016 Å
• c: 27.928 ± 0.005 Å
• α: 89.695 ± 0.003°
• β: 88.67 ± 0.003°
• γ: 83.918 ± 0.004°
• Cell volume: 2381.2 ± 0.7 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1245
• Residual factor for significantly intense reflections: 0.0534
• Weighted residual factors for significantly intense reflections: 0.0977
• Weighted residual factors for all reflections included in the refinement: 0.1222
• Goodness-of-fit parameter for all reflections included in the refinement: 1.038
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: Yes