Information card for entry 2022540

Structure parameters

• Chemical name: (μ~3~-η^6^:η^6^:η^6^-Anthracene)(μ~2~-η^6^:η^6^-anthracene)tris(tetrahydrofuran)sodiumdivanadium
• Formula: C40 H44 Na O3 V2
• Calculated formula: C40 H44 Na O3 V2
• Title of publication: Syntheses and crystal structures of new naphthalene– and anthracene–vanadate salts and an unprecedented dimetallabis(anthracene) sandwich complex: [Na(tetrahydrofuran)~3~][V~2~(anthracene)~2~]
• Authors of publication: Kucera, Benjamin E.; Young, Jr, Victor G.; Brennessel, William W.; Ellis, John E.
• Journal of publication: Acta Crystallographica Section C
• Year of publication: 2022
• Journal volume: 78
• Journal issue: 3
• a: 10.9951 ± 0.0016 Å
• b: 12.0777 ± 0.0018 Å
• c: 13.502 ± 0.002 Å
• α: 78.594 ± 0.003°
• β: 68.517 ± 0.003°
• γ: 78.738 ± 0.003°
• Cell volume: 1620.6 ± 0.4 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0882
• Residual factor for significantly intense reflections: 0.0438
• Weighted residual factors for significantly intense reflections: 0.099
• Weighted residual factors for all reflections included in the refinement: 0.1188
• Goodness-of-fit parameter for all reflections included in the refinement: 1.018
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: Yes